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Title5-(4-Cyano-5-dicyanomethylene-2,2-dimethyl-2,5-dihydro-3-furyl) -3-(1-methyl-1,4-dihydropyridin-4-ylidene)pent-4-enyl 3,5-bis-(benzyloxy) benzoate acetonitrile 0.25-solvate: A synchrotron radiation study
Publication TypeJournal Article
Year of Publication2009
AuthorsGainsford, G.J., Bhuiyan M.D.H., and Kay A.J.
JournalActa Crystallographica Section E: Structure Reports Online
Paginationo3261 - o3262
Date Published2009
ISSN16005368 (ISSN)
AbstractThe title compound, C42H36N4O 5·0.25CH3CN, crystallizes with a partial twofold disordered (1/4) acetonitrile solvent of crystallization. The linking atoms to the 3,5-bis-(benz-yloxy)benzoic acid are disordered between two conformations in the ratio 0.780 (6):0.220 (6). In the crystal, the mol-ecules pack using mainly C - H⋯N(cyano) inter-actions coupled with weak C - H⋯O(ether) inter-actions and C - H⋯π inter-actions. A brief comparison is made between a conventional and this synchrotron data collection.

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