| Title | 5-(4-Cyano-5-dicyanomethylene-2,2-dimethyl-2,5-dihydro-3-furyl) -3-(1-methyl-1,4-dihydropyridin-4-ylidene)pent-4-enyl 3,5-bis-(benzyloxy) benzoate acetonitrile 0.25-solvate: A synchrotron radiation study |
| Publication Type | Journal Article |
| Year of Publication | 2009 |
| Authors | Gainsford, G.J., Bhuiyan M.D.H., and Kay A.J. |
| Journal | Acta Crystallographica Section E: Structure Reports Online |
| Volume | 65 |
| Issue | 12 |
| Pagination | o3261 - o3262 |
| Date Published | 2009 |
| ISSN | 16005368 (ISSN) |
| Abstract | The title compound, C42H36N4O 5·0.25CH3CN, crystallizes with a partial twofold disordered (1/4) acetonitrile solvent of crystallization. The linking atoms to the 3,5-bis-(benz-yloxy)benzoic acid are disordered between two conformations in the ratio 0.780 (6):0.220 (6). In the crystal, the mol-ecules pack using mainly C - H⋯N(cyano) inter-actions coupled with weak C - H⋯O(ether) inter-actions and C - H⋯π inter-actions. A brief comparison is made between a conventional and this synchrotron data collection. |
| URL | http://www.scopus.com/inward/record.url?eid=2-s2.0-72049118833&partnerID=40&md5=2a3ccf0986e82dd224d0709442ddde48 |
| DOI | 10.1107/S1600536809050430 |
